(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

Base Information

Chemical Name:(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate
CAS No.:1430417-55-2
Molecular Formula:C₂₃H₂₄O₈
Molecular Weight:428.439
Hs Code.:

Synonyms:(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

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Technology Process of (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

There total 8 articles about (E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1430417-23-4
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-bis(tert-butyldimethylsilyloxy)phenyl)acrylate

: 1430417-55-2
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 331-39-5,501-16-6
caffeic acid

: 1430417-55-2
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

With dmap; tetrabutyl ammonium fluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ejmech.2012.09.047

Reference yield:

: 143815-52-5
(Z)-3-(3,4-dimethoxyphenyl)-2-hydroxyacrylic acid

: 1430417-55-2
(E)-1-(allyloxy)-3-(3,4-dimethoxyphenyl)-1-oxopropan-2-yl 3-(3,4-dihydroxyphenyl)acrylate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide; sodium tetrahydroborate / methanol / 0 - 20 °C / pH 10

2: toluene-4-sulfonic acid / toluene / 10 h / 100 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.ejmech.2012.09.047