[2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: [2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester
• CAS No.: 916084-77-0
• Molecular Formula: C₁₇H₂₇N₃O₃
• Molecular Weight: 321.42

Synonyms:[2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester

Chemical Property of [2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of [2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester

There total 2 articles about [2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-(Phenylacetyl)imidazole (55628-82-5) + [2-(2-amino-ethylamino)-ethyl]-carbamic acid tert-butyl ester (193206-49-4) → [2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester (916084-77-0)

Guidance literature:

In tetrahydrofuran;

Reference yield:

phenylacetic acid (103-82-2) → [2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester (916084-77-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran

2: tetrahydrofuran

In tetrahydrofuran;

DOI:10.1002/anie.200500842

Reference yield: 46.0%

[2-(2-phenylacetylamino-ethylamino)-ethyl]-carbamic acid tert-butyl ester (916084-77-0) + bis-(p-nitrophenyl) carbonate (5070-13-3) → (2-tert-butoxycarbonylamino-ethyl)-(2-phenylacetylamino-ethyl)-carbamic acid 4-nitro-phenyl ester (916084-78-1)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 0.166667h;

upstream raw materials:

1-(Phenylacetyl)imidazole

[2-(2-amino-ethylamino)-ethyl]-carbamic acid tert-butyl ester

phenylacetic acid

Downstream raw materials:

(2-tert-butoxycarbonylamino-ethyl)-(2-phenylacetylamino-ethyl)-carbamic acid 4-nitro-phenyl ester

[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamic acid 4-nitro-phenyl ester

[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamic acid 4-hydroxymethyl-phenyl ester

carbonic acid 4-[[2-(3-hydroxy-3-methyl-5-oxo-hexyloxycarbonylamino)-ethyl]-(2-phenylacetylamino-ethyl)-carbamoyloxy]-benzyl ester 4-nitro-phenyl ester

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