Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine

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Chemical Name:Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine
CAS No.:208584-90-1
Molecular Formula:C₃₆H₃₈BN₅O₃
Molecular Weight:599.54
Hs Code.:

Synonyms:Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine

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Chemical Property of Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine

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Technology Process of Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine

There total 6 articles about Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 138500-85-3
4-bromomethylphenylboronic acid pinacol ester

: 208584-80-9
Benzhydrylidene-[1-(4-methoxy-benzyl)-1H-tetrazol-5-ylmethyl]-amine

: 208584-90-1
Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 1.25h;
DOI:10.1016/S0040-4039(98)00492-4

Reference yield:

: 1013-88-3
Benzophenone imine

: 208584-90-1
Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) anh. HCl / 1.) MeOH; 2.) CH₂Cl₂, 16 h

2: 75 percent / NaHMDS / tetrahydrofuran / 1.25 h / -78 - 20 °C

With hydrogenchloride; sodium hexamethyldisilazane; In tetrahydrofuran;
DOI:10.1016/S0040-4039(98)00492-4

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 208584-90-1
Benzhydrylidene-{1-[1-(4-methoxy-benzyl)-1H-tetrazol-5-yl]-2-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-ethyl}-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 68 percent / sodium azide / acetic acid / 16 h / 40 °C

2: 89 percent / methanol / 3 h / Heating

3: 81 percent / hydrazine / ethanol / 16 h / Heating

4: 1.) anh. HCl / 1.) MeOH; 2.) CH₂Cl₂, 16 h

5: 75 percent / NaHMDS / tetrahydrofuran / 1.25 h / -78 - 20 °C

With hydrogenchloride; sodium azide; sodium hexamethyldisilazane; hydrazine; In tetrahydrofuran; methanol; ethanol; acetic acid;
DOI:10.1016/S0040-4039(98)00492-4