Technology Process of C72H68N6O8
There total 10 articles about C72H68N6O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,6-di-tert-butyl-4-methylpyridine; boron trichloride;
In
toluene;
at -78 ℃;
DOI:10.1021/ja0166141
- Guidance literature:
-
Multi-step reaction with 2 steps
1: DCC; HOAT / acetonitrile / 20 °C
2: 87 percent / BCl3; DTBMP / toluene / -78 °C
With
1-hydroxy-7-aza-benzotriazole; 2,6-di-tert-butyl-4-methylpyridine; boron trichloride; dicyclohexyl-carbodiimide;
In
toluene; acetonitrile;
DOI:10.1021/ja0166141
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: n-BuLi / tetrahydrofuran / -78 °C
1.2: MgBr2*OEt2 / tetrahydrofuran / -40 - 0 °C
1.3: 42 percent / tetrahydrofuran
2.1: 88 percent / PDC / acetonitrile / 20 °C
3.1: 90 percent / NaBH4 / methanol / -78 °C
4.1: 91 percent / Ph3P; DEAD; DPPA / toluene / 20 °C
5.1: 52 percent / Red-Al / toluene / 20 - 100 °C
6.1: NaNH2 / tetrahydrofuran / -78 °C
7.1: DCC; HOAT / acetonitrile / 20 °C
8.1: 87 percent / BCl3; DTBMP / toluene / -78 °C
With
sodium tetrahydroborate; dipyridinium dichromate; n-butyllithium; 1-hydroxy-7-aza-benzotriazole; 2,6-di-tert-butyl-4-methylpyridine; diphenyl-phosphinic acid; boron trichloride; sodium amide; dicyclohexyl-carbodiimide; triphenylphosphine; sodium bis(2-methoxyethoxy)aluminium dihydride; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; toluene; acetonitrile;
DOI:10.1021/ja0166141
