4-vinylbenzaldehyde diethyl acetal

Base Information

Chemical Name:4-vinylbenzaldehyde diethyl acetal
CAS No.:93429-66-4
Molecular Formula:C₁₃H₁₈O₂
Molecular Weight:206.285
Hs Code.:

Synonyms:4-vinylbenzaldehyde diethyl acetal

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Chemical Property of 4-vinylbenzaldehyde diethyl acetal

Chemical Property:

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Technology Process of 4-vinylbenzaldehyde diethyl acetal

There total 2 articles about 4-vinylbenzaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 81172-89-6
terephthalaldehyde mono(diethylacetal)

: 93429-66-4
4-vinylbenzaldehyde diethyl acetal

Guidance literature:: Methyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; at -78 - 25 ℃; for 1h;

terephthalaldehyde mono(diethylacetal); In tetrahydrofuran; at -78 - 25 ℃; for 5.5h;
DOI:10.1021/ja2120234

Reference yield:

: 93429-66-4
4-vinylbenzaldehyde diethyl acetal

Guidance literature:: /BRN= 99107/, /BRN= 697253/, THF, Rueckfluss, Ggw. von p-tert.-Butylbrenzcatechin;

Reference yield: 81.0%

: 55305-43-6
N-cyano-N-phenyl-p-toluenesulfonamide

: 93429-66-4
4-vinylbenzaldehyde diethyl acetal

: 73183-34-3
bis(pinacol)diborane

: 5-(diethoxymethyl)-2-(2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)ethyl)benzonitrile

Guidance literature:: bis(pinacol)diborane; With chloro[1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene]copper(I); lithium tert-butoxide; In tetrahydrofuran; at 20 ℃; for 0.5h; Glovebox; Molecular sieve; Inert atmosphere;

N-cyano-N-phenyl-p-toluenesulfonamide; 4-vinylbenzaldehyde diethyl acetal; In tetrahydrofuran; at 20 ℃; Glovebox; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201507303