2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Base Information

• Chemical Name: 2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide
• CAS No.: 1412405-59-4
• Molecular Formula: C₁₅H₁₉BrN₄OS
• Molecular Weight: 383.312

Synonyms:2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Chemical Property of 2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Chemical Property:

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Technology Process of 2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

There total 3 articles about 2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide (1412405-55-0) → 2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide (1412405-59-4)

Guidance literature:

With tert.-butylnitrite; copper(ll) bromide; In acetonitrile; at 20 ℃; for 2h;

Reference yield:

4-Isopropylaniline (99-88-7) → 2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide (1412405-59-4)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / 2 h

2: caesium carbonate / acetonitrile / 16 h

With caesium carbonate; triethylamine; In acetonitrile;

DOI:10.1016/j.bmcl.2014.04.081

Reference yield:

α-chloro-N-(p-isopropylphenyl)acetamide (1527-61-3) + C4H6BrN3S → 2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide (1412405-59-4)

Guidance literature:

With caesium carbonate; In acetonitrile; for 16h;

DOI:10.1016/j.bmcl.2014.04.081 DOI:10.1016/j.bmcl.2014.04.081

upstream raw materials:

2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

α-chloro-N-(p-isopropylphenyl)acetamide

4-Isopropylaniline

Downstream raw materials:

2-((4-ethyl-5-(2-fluoropyridin-4-yl)-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

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