2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Base Information

Chemical Name:2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide
CAS No.:1412405-55-0
Molecular Formula:C₁₅H₂₁N₅OS
Molecular Weight:319.431
Hs Code.:

Synonyms:2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

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Chemical Property of 2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Chemical Property:

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Technology Process of 2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

There total 1 articles about 2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-88-7
4-Isopropylaniline

: 17697-93-7
3-Amino-4-ethyl-5-mercapto-1,2,4-triazole

: 79-04-9
chloroacetyl chloride

: 1412405-55-0
2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Guidance literature:: 4-Isopropylaniline; chloroacetyl chloride; With triethylamine; In dichloromethane; for 2h;

3-Amino-4-ethyl-5-mercapto-1,2,4-triazole; With caesium carbonate; In acetonitrile; for 16h;

Reference yield:

: 1412405-55-0
2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

: 1412405-59-4
2-((5-bromo-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Guidance literature:: With tert.-butylnitrite; copper(ll) bromide; In acetonitrile; at 20 ℃; for 2h;

Reference yield:

: 1412405-55-0
2-((5-amino-4-ethyl-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

: 1412405-56-1
2-((4-ethyl-5-(2-fluoropyridin-4-yl)-4H-1,2,4-triazol-3-yl)thio)-N-(4-isopropylphenyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) bromide; tert.-butylnitrite / acetonitrile / 2 h / 20 °C

2: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; tetrahydrofuran / 0.75 h / 150 °C / Microwave irradiation

With tert.-butylnitrite; caesium carbonate; copper(ll) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; water; acetonitrile;