(10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone

Base Information

• Chemical Name: (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone
• CAS No.: 473574-28-6
• Molecular Formula: C₂₀H₁₆ClIN₂O₂
• Molecular Weight: 478.717

Synonyms:(10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone

Chemical Property of (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone

Chemical Property:

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Technology Process of (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone

There total 3 articles about (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxalyl dichloride (79-37-8) + 5-Chloro-4-iodo-2-methoxy-benzoic Acid (473264-13-0) + 10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine (22162-53-4) → (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone (473574-28-6)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

oxalyl dichloride (79-37-8) + 5-Chloro-4-iodo-2-methoxy-benzoic Acid (473264-13-0) + 3-methyl-N-(3-methylbutyl)-1-butanamine (544-00-3) + 10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine (22162-53-4) → (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone (473574-28-6)

Guidance literature:

In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

3-methyl-N-(3-methylbutyl)-1-butanamine (544-00-3) + 10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine (22162-53-4) → (10,11-Dihydro-5H-pyrrolo[2,1-c][1,4]benzodiazepin-10-yl)-(2-methoxy-4-iodo-5-chlorophenyl)-methanone (473574-28-6) + 10-(5-Chloro-4-cyclohex-1-en-1-yl-2-me3thoxybenzoyl)-N-methyl-N-(pyridin-3-ylmethyl)-10,11-dihydro-5H-pyrrolo [2,1-c][1,4]benzodiazepine-3-carboxamide

Guidance literature:

In dichloromethane;

upstream raw materials:

oxalyl dichloride

5-Chloro-4-iodo-2-methoxy-benzoic Acid

3-methyl-N-(3-methylbutyl)-1-butanamine

10,11-dihydro-5H-benzo[e]pyrrolo[1,2-a][1,4]diazepine

Downstream raw materials:

(10,11-Dihydro-5H-pyrrolo [2,1-c][1,4] benzodiazepin-10-yl)-[5-chloro-2-methoxy-4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-methanone

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