4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide

Base Information

Chemical Name:4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide
CAS No.:1620558-00-0
Molecular Formula:C₁₅H₁₄N₆O₃S
Molecular Weight:358.381
Hs Code.:

Synonyms:4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide

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Technology Process of 4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide

There total 5 articles about 4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.2%

: 1620557-99-4
methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

: 1620558-00-0
4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Reflux;
DOI:10.1016/j.ejmech.2014.06.049

Reference yield:

: 1620557-98-3
4-[2-(5-oxo-2-phenyl-4,5-dihydro-1,3-oxazol-4-yliden)hydrazino]-1-benzenesulfonamide

: 1620558-00-0
4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / methanol / 1 h / 20 °C

2: hydrazine hydrate / ethanol / 6 h / Reflux

With hydrazine hydrate; potassium hydroxide; In methanol; ethanol;
DOI:10.1016/j.ejmech.2014.06.049

Reference yield:

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 1620558-00-0
4-[3-(hydrazinocarbonyl)-5-phenyl-1H-1,2,4-triazol-1-yl]-1-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic anhydride / 80 °C

2.1: sodium nitrite; hydrogenchloride / water / 0.25 h / 0 - 5 °C

2.2: 4 h / 0 - 5 °C

3.1: potassium hydroxide / methanol / 1 h / 20 °C

4.1: hydrazine hydrate / ethanol / 6 h / Reflux

With hydrogenchloride; acetic anhydride; hydrazine hydrate; potassium hydroxide; sodium nitrite; In methanol; ethanol; water;
DOI:10.1016/j.ejmech.2014.06.049