methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

Base Information

Chemical Name:methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate
CAS No.:1620557-99-4
Molecular Formula:C₁₆H₁₄N₄O₄S
Molecular Weight:358.378
Hs Code.:

Synonyms:methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

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Chemical Property of methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

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Technology Process of methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

There total 4 articles about methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1620557-98-3
4-[2-(5-oxo-2-phenyl-4,5-dihydro-1,3-oxazol-4-yliden)hydrazino]-1-benzenesulfonamide

: 1620557-99-4
methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

Guidance literature:: With potassium hydroxide; In methanol; at 20 ℃; for 1h;
DOI:10.1016/j.ejmech.2014.06.049

Reference yield:

: 495-69-2,140480-84-8,21251-67-2,91787-63-2,66407-11-2
Hippuric Acid

: 1620557-99-4
methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic anhydride / 80 °C

2.1: sodium nitrite; hydrogenchloride / water / 0.25 h / 0 - 5 °C

2.2: 4 h / 0 - 5 °C

3.1: potassium hydroxide / methanol / 1 h / 20 °C

With hydrogenchloride; acetic anhydride; potassium hydroxide; sodium nitrite; In methanol; water;
DOI:10.1016/j.ejmech.2014.06.049

Reference yield:

: 1199-01-5,53766-22-6
2-phenylazlactone

: 1620557-99-4
methyl 1-[4-(aminosulfonyl)phenyl]-5-phenyl-1H-1,2,4-triazole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / water / 0.25 h / 0 - 5 °C

1.2: 4 h / 0 - 5 °C

2.1: potassium hydroxide / methanol / 1 h / 20 °C

With hydrogenchloride; potassium hydroxide; sodium nitrite; In methanol; water;
DOI:10.1016/j.ejmech.2014.06.049