1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide

Base Information

• Chemical Name: 1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide
• CAS No.: 123484-51-5
• Molecular Formula: Br₃*C₁₄H₁₆BrN₂S
• Molecular Weight: 563.976

Synonyms:1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide

Chemical Property of 1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide

Chemical Property:

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Technology Process of 1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide

There total 1 articles about 1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

acetone (67-64-1) → 1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide (123484-51-5) + 1-bromoacetone (598-31-2)

Guidance literature:

With 4-bromo-6,8-dimethyl-9-cyano-4a,10a-cis-4,4a-trans-1,2,3,4,4a,10a-hexahydrobenzothiazolo<3,2-a>pyridinium bromide; bromine; for 0.5h;

DOI:10.1007/BF00486687

Reference yield: 72.0%

1,3-dimethyl-4-cyano-5a,9a-cis-9,9a-trans-6,7,8,9,5a,9a-hexahydrobenzothiazolo<3,2-a>pyridinium tribromide (123484-51-5) → 4-bromo-6,8-dimethyl-9-cyano-4a,10a-cis-4,4a-trans-1,2,3,4,4a,10a-hexahydrobenzothiazolo<3,2-a>pyridinium bromide (121567-81-5) + 1-bromoacetone (598-31-2)

Guidance literature:

With acetone; at 25 ℃; for 0.333333h;

DOI:10.1007/BF00486687

upstream raw materials:

acetone

Downstream raw materials:

4-bromo-6,8-dimethyl-9-cyano-4a,10a-cis-4,4a-trans-1,2,3,4,4a,10a-hexahydrobenzothiazolo<3,2-a>pyridinium bromide

1-bromoacetone

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