C₂₂H₃₂N₂O₅

Base Information

Chemical Name:C₂₂H₃₂N₂O₅
CAS No.:1421747-61-6
Molecular Formula:C₂₂H₃₂N₂O₅
Molecular Weight:404.506
Hs Code.:

C<sub>22</sub>H<sub>32</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₂H₃₂N₂O₅

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Chemical Property of C₂₂H₃₂N₂O₅

Chemical Property:

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Technology Process of C₂₂H₃₂N₂O₅

There total 11 articles about C₂₂H₃₂N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110769-87-4
C₁₁H₁₃NO₂*C₁₈H₁₄O₈

: 66866-44-2
Boc-Leu-O-COO-isoBu

: 1421747-61-6
C₂₂H₃₂N₂O₅

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at -15 - 20 ℃; for 5.25h;
DOI:10.1016/j.bmc.2012.11.046

Reference yield:

: 3092-20-4
diethyl 2-phenylcyclopropane-1,1-dicarboxylate

: 1421747-61-6
C₂₂H₃₂N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide / methanol; water / 12 h / 20 °C

2.1: sodium hydroxide / ethanol / 1 h / 20 °C

2.2: 18 h / Reflux

3.1: sulfuric acid; sodium nitrite / water / 2 h / 0 °C

5.1: 10 h / Reflux

6.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

7.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

7.2: 12 h / 20 °C

8.1: triethylamine / dichloromethane; tetrahydrofuran / 5.25 h / -15 - 20 °C

With hydrogenchloride; sulfuric acid; triethylamine; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.bmc.2012.11.046

Reference yield:

: 5292-53-5
diethyl benzalmalonate

: 1421747-61-6
C₂₂H₃₂N₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil; tetrahydrofuran / 1.17 h / 20 - 50 °C

2.1: sodium hydroxide / methanol; water / 12 h / 20 °C

3.1: sodium hydroxide / ethanol / 1 h / 20 °C

3.2: 18 h / Reflux

4.1: sulfuric acid; sodium nitrite / water / 2 h / 0 °C

6.1: 10 h / Reflux

7.1: hydrogenchloride / ethyl acetate / 3 h / 20 °C

8.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

8.2: 12 h / 20 °C

9.1: triethylamine / dichloromethane; tetrahydrofuran / 5.25 h / -15 - 20 °C

With hydrogenchloride; sulfuric acid; sodium hydride; triethylamine; sodium hydroxide; sodium nitrite; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; mineral oil;
DOI:10.1016/j.bmc.2012.11.046