4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

Base Information

Chemical Name:4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene
CAS No.:142706-75-0
Molecular Formula:C₁₄H₆F₁₅NO₃
Molecular Weight:521.183
Hs Code.:

Synonyms:4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

Suppliers and Price of 4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

There total 4 articles about 4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 17352-09-9
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-n-octyl trifluoromethanesulfonate

: 142706-75-0
4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

Guidance literature:: With sodium hydride; In N,N,N,N,N,N-hexamethylphosphoric triamide; 1.) r.t., 2.) 110 deg C, 8 h;
DOI:10.1016/S0022-1139(96)03490-2

Reference yield: 89.0%

: 100-25-4
para-dinitrobenzene

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

: 142706-75-0
4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

Guidance literature:: With tetrabutyl ammonium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/jo048354m

Reference yield: 45.0%

: 636-98-6
p-nitrobenzene iodide

: 307-30-2
2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-1-octanol

: 142706-75-0
4-nitro-1-(2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluorooctyloxy)benzene

Guidance literature:: With copper(l) iodide; caesium carbonate; ethyl 2-oxocyclohexane carboxylate; for 17h; Neat (no solvent); Reflux;
DOI:10.1002/ejoc200900303