2,3,4,5-tetramethoxyaniline

Base Information

Chemical Name:2,3,4,5-tetramethoxyaniline
CAS No.:142004-02-2
Molecular Formula:C₁₀H₁₅NO₄
Molecular Weight:213.233
Hs Code.:

Synonyms:2,3,4,5-tetramethoxyaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,4,5-tetramethoxyaniline

Chemical Property:

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Technology Process of 2,3,4,5-tetramethoxyaniline

There total 3 articles about 2,3,4,5-tetramethoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 142004-01-1
1-nitro-2,3,4,5-tetramethoxybenzene

: 142004-02-2
2,3,4,5-tetramethoxyaniline

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 1h; under 2068.6 Torr;
DOI:10.1021/jm00092a022

Reference yield:

: 52978-83-3
2,3,4-trimethoxy-6-nitrobenzaldehyde

: 142004-02-2
2,3,4,5-tetramethoxyaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) m-chloroperbenzoic acid, 2.) KOH / 1.) CHCl₃, reflux, 5 h, 2.) H₂O, MeOH, RT

2: 71 percent / diethyl ether / 4 h / Ambient temperature

3: 87 percent / H₂ / 10percent Pd/C / ethanol / 1 h / 2068.6 Torr

With potassium hydroxide; hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jm00092a022

Reference yield:

: 142004-00-0
2-hydroxy-1-nitro-3,4,5-trimethoxybenzene

: 142004-02-2
2,3,4,5-tetramethoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / diethyl ether / 4 h / Ambient temperature

2: 87 percent / H₂ / 10percent Pd/C / ethanol / 1 h / 2068.6 Torr

With hydrogen; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jm00092a022