benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside
CAS No.:102794-16-1
Molecular Formula:C₂₂H₂₅Cl₆NO₉
Molecular Weight:660.16
Hs Code.:

Synonyms:benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

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Chemical Property of benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

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Technology Process of benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

There total 1 articles about benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 102794-17-2
benzyl 2-amino-2-deoxy-4,6-O-isopropylidene-β-D-glucopyranoside

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 102794-16-1
benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: With dmap; for 2h; Ambient temperature;
DOI:10.1248/cpb.33.4098

Reference yield: 99.0%

: 102794-16-1
benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

: 114827-03-1,102794-18-3
benzyl 2-deoxy-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

Guidance literature:: With acetic acid; In water; at 85 - 90 ℃; for 0.25h;
DOI:10.1248/cpb.35.4517

Reference yield:

: 102794-16-1
benzyl 2-deoxy-4,6-O-isopropylene-2-<(2,2,2-trichloroethoxycarbonyl)amino>-3-O-(2,2,2-trichloroethoxycarbonyl)-β-D-glucopyranoside

: (R)-3-Dodecyloxy-tetradecanoic acid (2R,3S,4R,5R)-3-(diphenoxy-phosphoryloxy)-5-((R)-3-dodecyloxy-tetradecanoylamino)-6-hydroxy-2-hydroxymethyl-tetrahydro-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 98 percent / 90percent acetic acid / H₂O / 0.25 h / 90 °C

2: 85 percent / tetramethylurea / CH₂Cl₂ / 16 h / Ambient temperature

3: 87 percent / pyridine, 4-dimethylaminopyridine / benzene / 2 h / Ambient temperature

4: 96 percent / zinc / acetic acid / 5 h / Ambient temperature

5: 68 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 0 - 5 °C

6: dicyclohexylcarbodiimide, 4-dimethylaminopyridine / CH₂Cl₂ / 16 h / Ambient temperature

7: 1.) 10percent Pd-on-carbon; 2.) PtO₂ / 1.) 45 degC, 5 h; 2.) methanol, 16 h, r.t.

With pyridine; dmap; acetic acid; dicyclohexyl-carbodiimide; tetramethylurea; zinc; platinum(IV) oxide; palladium on activated charcoal; In dichloromethane; water; acetic acid; benzene;
DOI:10.1248/cpb.33.4098