methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate

Base Information

Chemical Name:methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate
CAS No.:725229-85-6
Molecular Formula:C₂₅H₃₁N₃O₃
Molecular Weight:421.539
Hs Code.:

Synonyms:methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate

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Chemical Property of methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate

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Technology Process of methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate

There total 1 articles about methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 79-22-1
methyl chloroformate

: 725229-84-5
4-[(3-aminophenyl)[4-[(diethylamino)carbonyl]phenyl]methylene]-1-piperidinecarboxylic acid, 1,1-dimethylethyl ester

: 725229-85-6
methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate

Guidance literature:: methyl chloroformate; With zinc; In toluene; for 0.166667h;

4-[(3-aminophenyl)[4-[(diethylamino)carbonyl]phenyl]methylene]-1-piperidinecarboxylic acid, 1,1-dimethylethyl ester; In dichloromethane; toluene; at 20 ℃; for 24h;

With sodium hydrogencarbonate; trifluoroacetic acid; more than 3 stages;

Reference yield: 54.0%

: 725229-85-6
methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate

: 107-08-4
1-iodo-propane

: 76-05-1
trifluoroacetic acid

: methyl [3-[[4-[(diethylamino)carbonyl]phenyl](1-propyl-4-piperidinylidene)methyl]phenyl]carbamate trifluoroacetate

Guidance literature:: methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate; 1-iodo-propane; With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 15h;

trifluoroacetic acid; In water; acetonitrile;

Reference yield: 34.0%

: 725229-85-6
methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate

: 76-05-1
trifluoroacetic acid

: 1489-69-6
Cyclopropanecarboxaldehyde

: methyl [3-[[1-(cyclopropylmethyl)-4-piperidinylidene][4-(diethylamino)carbonyl]phenyl]methylphenyl]carbamate trifluoroacetate

Guidance literature:: methyl 3-[{4-[(diethylamino)carbonyl]phenyl}(piperidin-4-ylidene)methyl]phenylcarbamate; Cyclopropanecarboxaldehyde; With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 15h;

trifluoroacetic acid; In dichloromethane; for 0.5h;