tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate

Base Information

Chemical Name:tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate
CAS No.:1453219-61-8
Molecular Formula:C₁₆H₃₆N*C₃₅H₂₀BF₂₂N₂
Molecular Weight:1139.8
Hs Code.:

Synonyms:tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate

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Technology Process of tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate

There total 3 articles about tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110-85-0
piperazine

: 1013095-39-0
tetrabutylammonium (4-bromomethyl-2,3,5,6-tetrafluorophenyl)tris[3,5-bis(trifluoromethyl)phenyl]borate

: 1453219-61-8
tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate

Guidance literature:: In tetrahydrofuran; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201202408

Reference yield: 73.0%

: 1013095-39-0
tetrabutylammonium (4-bromomethyl-2,3,5,6-tetrafluorophenyl)tris[3,5-bis(trifluoromethyl)phenyl]borate

: 74-89-5
methylamine

: 1453219-61-8
tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 3h; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201202408

Reference yield:

: 1013095-35-6
tetrabutylammonium (2,3,5,6-tetrafluoro-4-hydroxymethylphenyl)tris[3,5-bis(trifluoromethyl)phenyl]borate

: 1453219-61-8
tetrabutylammonium [2,3,5,6-tetrafluoro-4-(methylaminomethyl)phenyl]tris[3,5-bis(trifluoromethyl)phenyl]borate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide; tetrabutylammomium bromide / dichloromethane / 20 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2: tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

With tetrabutylammomium bromide; phosphorus tribromide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201202408