dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside
CAS No.:212713-50-3
Molecular Formula:C₂₄H₃₆Cl₃NO₇Si
Molecular Weight:584.997
Hs Code.:

Synonyms:dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

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Chemical Property of dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

There total 1 articles about dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: {(2S,3R,4R,5S,6R)-2-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl}-carbamic acid 2,2,2-trichloro-ethyl ester

: 212713-50-3
dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetonitrile; at 20 ℃; for 8h;
DOI:10.1002/ejoc.200900973

Reference yield: 95.0%

: 212713-50-3
dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

: 123-76-2
levulinic acid

: 1400594-72-0
dimethylthexylsilyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-(2,2,2-trichloroethoxy)carbonylamino-β-D-glucopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/ja3069962

Reference yield: 80.0%

: 91681-56-0
(3R)-3-dodecanoyloxytetradecanoic acid

: 212713-50-3
dimethylthexylsilyl 4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

: 1214268-20-8
dimethylthexylsilyl 3-O-[(R)-3-(dodecanoyloxy)tetradecanoyl]-4,6-O-benzylidene-2-[(2,2,2-trichloroethoxy)carbonylamino]-2-deoxy-β-D-glucopyranoside

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1002/ejoc.200900973