Diethylene glycol, decyl ether

Base Information

• Chemical Name: Diethylene glycol, decyl ether
• CAS No.: 23238-41-7
• Molecular Formula: C14H30 O3
• Molecular Weight: 246.39
• Hs Code.: 2909499000
• DSSTox Substance ID: DTXSID201025081
• Nikkaji Number: J1.439.460E
• Mol file: 23238-41-7.mol

Synonyms:Diethylene glycol, decyl ether;2-(2-decoxyethoxy)ethanol;2-(2-decyloxy-ethoxy)-ethanol;diethyleneglycol decyl ether;3,6-Dioxahexadecane-1-ol;23238-41-7;SCHEMBL1085931;2-(2-(decyloxy)ethoxy)ethanol;C10-AEO-2;2-[2-(decyloxy)ethoxy]-ethanol;DTXSID201025081;AKOS024390782

Chemical Property of Diethylene glycol, decyl ether

Chemical Property:

• Vapor Pressure: 5.79E-06mmHg at 25°C
• Refractive Index: n20/D 1.445
• Boiling Point: 340.2°C at 760 mmHg
• Flash Point: 159.6°C
• PSA: 38.69000
• Density: 0.911 g/mL at 20 °C(lit.)
• LogP: 3.15260
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 14
• Exact Mass: 246.21949481
• Heavy Atom Count: 17
• Complexity: 129

Purity/Quality:

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCOCCOCCO

Technology Process of Diethylene glycol, decyl ether

There total 3 articles about Diethylene glycol, decyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

decyl chloride (1002-69-3) + diethylene glycol (111-46-6) → 1-Decanol (112-30-1) + 1-Decene (872-05-9,17438-89-0,25189-70-2) + 2-<2-decyloxy)ethoxy>ethanol (23238-41-7)

Guidance literature:

With sodium hydroxide; water; at 100 ℃; for 24h; Yields of byproduct given;

DOI:10.1021/jo01294a034

Reference yield: 79.0%

1-bromo dodecane (112-29-8) + diethylene glycol (111-46-6) → 1-Decanol (112-30-1) + 1-Decene (872-05-9,17438-89-0,25189-70-2) + 2-<2-decyloxy)ethoxy>ethanol (23238-41-7)

Guidance literature:

With sodium hydroxide; water; at 100 ℃; for 24h; Yields of byproduct given;

DOI:10.1021/jo01294a034

Reference yield: 21.0%

1-bromo dodecane (112-29-8) + diethylene glycol (111-46-6) → 1-Decanol (112-30-1) + 1-Decene (872-05-9,17438-89-0,25189-70-2) + 2-<2-decyloxy)ethoxy>ethanol (23238-41-7) + diethylene glycol didecyl ether (72659-41-7)

Guidance literature:

With sodium hydroxide; water; at 100 ℃; for 24h;

DOI:10.1021/jo01294a034

upstream raw materials:

decyl chloride

diethylene glycol

1-bromo dodecane

Downstream raw materials:

4-hydroxy-N,N,N-trimethyl-7-(phenylmethoxy)-3,5,9,12,15-pentaoxa-4-phosphapentacosan-1-aminium, 4-oxide, hydroxide, inner salt

Phosphoric acid 2-benzyloxy-3-[2-(2-decyloxy-ethoxy)-ethoxy]-propyl ester 2-bromo-ethyl ester

3-<2-<2-(decyloxy)ethoxy>ethoxy>-2-(phenylmethoxy)-1-propanol

1-[2-[2-(decyloxy)ethoxy]ethoxy]-3-[(4-methoxyphenyl)diphenylmethoxy]-2-propanol

Refernces