N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine

Base Information

• Chemical Name: N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine
• CAS No.: 55723-80-3
• Molecular Formula: C₄H₄Cl₃N₃S₂
• Molecular Weight: 264.587

Synonyms:N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine

Chemical Property of N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine

Chemical Property:

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Technology Process of N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine

There total 1 articles about N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-1,2,4-thiadiazol-5-amine (17467-35-5) + chlorothio-trichloro-methane (594-42-3) → N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine (55723-80-3)

Guidance literature:

In methanol;

DOI:10.1021/jo00906a006

Reference yield:

3-nitro-aniline (99-09-2) + N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine (55723-80-3) → (3-methyl-[1,2,4]thiadiazolo[5,4-c][1,2,4]thiadiazol-5-ylidene)-(3-nitro-phenyl)-amine (55723-75-6)

Guidance literature:

With triethylamine; In chloroform;

DOI:10.1021/jo00906a006

Reference yield:

2,5 dichloroaniline (95-82-9) + N-(3-methyl-[1,2,4]thiadiazol-5-yl)-S-trichloromethyl-thiohydroxylamine (55723-80-3) → (2,5-dichloro-phenyl)-(3-methyl-[1,2,4]thiadiazolo[5,4-c][1,2,4]thiadiazol-5-ylidene)-amine (55723-74-5)

Guidance literature:

With triethylamine; In chloroform;

DOI:10.1021/jo00906a006

upstream raw materials:

3-methyl-1,2,4-thiadiazol-5-amine

chlorothio-trichloro-methane

Downstream raw materials:

(3-methyl-[1,2,4]thiadiazolo[5,4-c][1,2,4]thiadiazol-5-ylidene)-(3-nitro-phenyl)-amine

(2,5-dichloro-phenyl)-(3-methyl-[1,2,4]thiadiazolo[5,4-c][1,2,4]thiadiazol-5-ylidene)-amine

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