2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol

Base Information

Chemical Name:2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol
CAS No.:1352447-37-0
Molecular Formula:C₁₈H₂₆O₇
Molecular Weight:354.4
Hs Code.:

Synonyms:2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol

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Chemical Property of 2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol

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Technology Process of 2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol

There total 6 articles about 2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₈H₂₄O₇

: 1352447-37-0
2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol

Guidance literature:: C₁₈H₂₄O₇; With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;

With ammonium chloride; In methanol; Saturated solution;
DOI:10.1016/j.tet.2011.10.063

Reference yield:

: C₁₉H₂₈O₈

: 1352447-37-0
2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium periodate / dichloromethane; water / 3 h / 20 °C

2.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

2.2: Saturated solution

With sodium tetrahydroborate; sodium periodate; In methanol; dichloromethane; water;
DOI:10.1016/j.tet.2011.10.063

Reference yield:

: 1352447-35-8
((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyl-tetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methanol

: 1352447-37-0
2-(((3aR,4R,6R,6aR)-6-(4-methoxybenzyloxy)-2,2-dimethyltetrahydrofuro[3,4-d]-[1,3]dioxol-4-yl)methoxy)ethanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil

1.2: 12 h / 20 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water / 20 °C

3.1: sodium periodate / dichloromethane; water / 3 h / 20 °C

4.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

4.2: Saturated solution

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.tet.2011.10.063