meso-Bis--disiloxan

Base Information

• Chemical Name: meso-Bis--disiloxan
• CAS No.: 18876-52-3
• Molecular Formula: C₃₄H₃₀OSi₂
• Molecular Weight: 510.783

Synonyms:meso-Bis--disiloxan

Chemical Property of meso-Bis--disiloxan

Chemical Property:

Purity/Quality:

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Technology Process of meso-Bis--disiloxan

There total 3 articles about meso-Bis--disiloxan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

S(-)-methyl-α-naphthyl-phenyl-chlorosilane (960-82-7) → meso-Bis--disiloxan (18876-52-3)

Guidance literature:

With lead(II) oxide; In ethyl acetate; for 48h; Heating;

DOI:10.1021/ol990068n

Reference yield:

chloro-diphenylphosphine (1079-66-9,74391-44-9) + potassium naphthylphenylmethylsilanolate (3554-09-4,18142-89-7,107487-20-7) → meso-Bis--disiloxan (18876-52-3) + tetraphenyldiphosphine oxide (2096-83-5)

Guidance literature:

In 1,4-dioxane; -50 deg C;

DOI:10.1016/S0040-4020(01)89077-3

Reference yield:

→ meso-Bis--disiloxan (18876-52-3)

Guidance literature:

Aus R3SiCl;

upstream raw materials:

chloro-diphenylphosphine

potassium naphthylphenylmethylsilanolate

S(-)-methyl-α-naphthyl-phenyl-chlorosilane

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