(6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone

Base Information

Chemical Name:(6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone
CAS No.:1300690-14-5
Molecular Formula:C₃₂H₂₅Br₂NO₆
Molecular Weight:679.362
Hs Code.:

Synonyms:(6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone

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Chemical Property of (6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone

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Technology Process of (6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone

There total 4 articles about (6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1300690-12-3
6-bromo-2-methoxy-1-naphthoyl chloride

: 79257-61-7
N-(3,5-dimethoxy-phenyl)-acetamide

: 1300690-13-4
(6-bromo-2-methoxynaphth-1-yl)-(2-acetamido-4,6-dimethoxyphenyl)ketone

: 1300690-14-5
(6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone

Guidance literature:: 6-bromo-2-methoxy-1-naphthoyl chloride; With tin(IV) chloride; In 1,2-dichloro-ethane; at 45 ℃; for 0.5h;

N-(3,5-dimethoxy-phenyl)-acetamide; In 1,2-dichloro-ethane; at 45 ℃; for 20h;
DOI:10.1016/j.ejmech.2011.02.050

Reference yield:

: 5111-65-9
2-Bromo-6-methoxynaphthalene

: 1300690-13-4
(6-bromo-2-methoxynaphth-1-yl)-(2-acetamido-4,6-dimethoxyphenyl)ketone

: 1300690-14-5
(6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / toluene / 5 h / 100 °C

2.1: potassium permanganate / water; acetone / 4 h / 70 °C

2.2: pH 10

2.3: pH 2

3.1: thionyl chloride / 3 h / 65 °C

4.1: tin(IV) chloride / 1,2-dichloro-ethane / 0.5 h / 45 °C

4.2: 20 h / 45 °C

With potassium permanganate; thionyl chloride; tin(IV) chloride; trichlorophosphate; In water; 1,2-dichloro-ethane; acetone; toluene; 4.1: Friedel-Crafts acylation / 4.2: Friedel-Crafts acylation;
DOI:10.1016/j.ejmech.2011.02.050

Reference yield:

: 247174-18-1
6-bromo-2-methoxynaphthalene-1-carbaldehyde

: 1300690-13-4
(6-bromo-2-methoxynaphth-1-yl)-(2-acetamido-4,6-dimethoxyphenyl)ketone

: 1300690-14-5
(6-bromo-2-methoxynaphth-1-yl)[2-(6-bromo-2-methoxy-1-naphthoylamino)-4,6-dimethoxyphenyl]ketone

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium permanganate / water; acetone / 4 h / 70 °C

1.2: pH 10

1.3: pH 2

2.1: thionyl chloride / 3 h / 65 °C

3.1: tin(IV) chloride / 1,2-dichloro-ethane / 0.5 h / 45 °C

3.2: 20 h / 45 °C

With potassium permanganate; thionyl chloride; tin(IV) chloride; In water; 1,2-dichloro-ethane; acetone; 3.1: Friedel-Crafts acylation / 3.2: Friedel-Crafts acylation;
DOI:10.1016/j.ejmech.2011.02.050