3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide

Base Information

Chemical Name:3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide
CAS No.:1416916-78-3
Molecular Formula:C₂₂H₃₇NO₃S
Molecular Weight:395.607
Hs Code.:

Synonyms:3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide

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Technology Process of 3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide

There total 1 articles about 3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 73604-46-3
2,2-dimethyl-1-amino-pent-4-ene

: 160252-94-8
3,5-di-tert-butyl-4-methoxybenzene-1-sulfonyl chloride

: 1416916-78-3
3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/jo3023632

Reference yield: 88.0%

: 2564-83-2
2,2,6,6-tetramethyl-piperidine-N-oxyl

: 1416916-78-3
3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide

: 1416916-82-9
(S)-1-((1-((3,5-di-tert-butyl-4-methoxyphenyl)sulfonyl)-4,4-dimethylpyrrolidin-2-yl)methoxy)-2,2,6,6-tetramethylpiperidine

Guidance literature:: With α,α,α-trifluorotoluene; oxygen; copper(II) bis(trifluoromethanesulfonate); potassium carbonate; (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); at 20 - 110 ℃; for 6h; under 760.051 Torr; enantioselective reaction;
DOI:10.1021/jo3023632

Reference yield: 54.0%

: 1416916-78-3
3,5-di-tert-butyl-N-(2,2-dimethylpent-4-en-1-yl)-4-methoxybenzenesulfonamide

: 1-((3,5-di-tert-butyl-4-methoxyphenyl)sulfonyl)-4,4-dimethylpyrrolidine-2-carbaldehyde

Guidance literature:: With oxygen; copper(l) chloride; In toluene; at 120 ℃; for 12h; under 760.051 Torr; chemoselective reaction; Molecular sieve;
DOI:10.1021/jacs.7b05680