2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid

Base Information

Chemical Name:2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid
CAS No.:112800-52-9
Molecular Formula:C₁₈H₂₁NO₄S
Molecular Weight:347.435
Hs Code.:

Synonyms:2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid

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Chemical Property of 2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid

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Technology Process of 2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid

There total 1 articles about 2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 6723-30-4
O-2-tetrahydro-2H-pyranhydroxylamine

: 89008-59-3
2-Hydroxy-3-phenyl-2-(2-thienyl)propansaeure

: 112800-52-9
2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid

Guidance literature:: With 1,1'-carbonyldiimidazole; In dichloromethane;
DOI:10.1002/ardp.19873200813

Reference yield: 43.0%

: 112800-52-9
2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid

: 112800-41-6
5,6-Dihydro-6-(phenylmethyl)-4-(tetrahydro-2H-2-pyranyloxy)-4H-thieno<3,2-b>pyrrol-5-on

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrachloromethane; at 76 ℃; for 14h;
DOI:10.1002/ardp.19873200813

Reference yield:

: 112800-52-9
2-Hydroxy-3-phenyl-N-(tetrahydro-2H-2-pyranyloxy)-2-(2-thienyl)propanamid

: 5,6-Dihydro-6-(phenylmethyl)-4H-thieno<3,2-b>pyrrol-5-on

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / dicyclohexylcarbodiimide / CCl₄ / 14 h / 76 °C

2: 72 percent / Lewatit S 100 / methanol / Heating

With Lewatit S 100; dicyclohexyl-carbodiimide; In methanol; tetrachloromethane;
DOI:10.1002/ardp.19873200813