(1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone

Base Information

Chemical Name:(1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone
CAS No.:1610565-63-3
Molecular Formula:C₂₇H₂₃ClN₂O
Molecular Weight:426.945
Hs Code.:

Synonyms:(1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone

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Chemical Property of (1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone

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Technology Process of (1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone

There total 4 articles about (1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: bis(4-chlorophenyl)iodonium tetrafluoroborate

: 2-isocyano-3,3-diphenyl-1-(piperidin-1-yl)prop-2-en-1-one

: 1610565-63-3
(1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone

Guidance literature:: With tris[2-phenylpyridinato-C²,N]iridium(III); sodium carbonate; In methanol; at 26 ℃; for 24h; Inert atmosphere; Irradiation;
DOI:10.1039/c4cc01122h

Reference yield:

: 119-61-9
benzophenone

: 1610565-63-3
(1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C

2: triethylamine; trichlorophosphate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3: tris[2-phenylpyridinato-C²,N]iridium(III); sodium carbonate / methanol / 24 h / 26 °C / Inert atmosphere; Irradiation

With tris[2-phenylpyridinato-C²,N]iridium(III); sodium hydride; sodium carbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1039/c4cc01122h

Reference yield:

: 67434-28-0
2-isocyano-1-(piperidin-1-yl) ethan-1-one

: 1610565-63-3
(1-(4-chlorophenyl)-4-phenylisoquinolin-3-yl)(piperidin-1-yl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / mineral oil; tetrahydrofuran / 2 h / 20 °C

2: triethylamine; trichlorophosphate / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3: tris[2-phenylpyridinato-C²,N]iridium(III); sodium carbonate / methanol / 24 h / 26 °C / Inert atmosphere; Irradiation

With tris[2-phenylpyridinato-C²,N]iridium(III); sodium hydride; sodium carbonate; triethylamine; trichlorophosphate; In tetrahydrofuran; methanol; mineral oil;
DOI:10.1039/c4cc01122h