C₂₃H₂₆N₂O₄

Base Information

Chemical Name:C₂₃H₂₆N₂O₄
CAS No.:1379591-15-7
Molecular Formula:C₂₃H₂₆N₂O₄
Molecular Weight:394.47
Hs Code.:

C<sub>23</sub>H<sub>26</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₃H₂₆N₂O₄

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Chemical Property of C₂₃H₂₆N₂O₄

Chemical Property:

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Technology Process of C₂₃H₂₆N₂O₄

There total 8 articles about C₂₃H₂₆N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1379591-92-0
(2E,4E)-N-methyI-7-phenylhepta-2,4-dien-1-amine hydrochloride

: 13683-89-1
methyl N-(3-hydroxyphenyl)carbamate

: 7693-46-1
4-Nitrophenyl chloroformate

: 1379591-15-7
C₂₃H₂₆N₂O₄

Guidance literature:: methyl N-(3-hydroxyphenyl)carbamate; 4-Nitrophenyl chloroformate; With triethylamine; In tetrahydrofuran; at 20 ℃; for 2h;

(2E,4E)-N-methyI-7-phenylhepta-2,4-dien-1-amine hydrochloride; With triethylamine; In tetrahydrofuran; at 60 ℃; for 15h;

Reference yield:

: 477531-94-5
(2E,4E)-ethyl 7-phenylhepta-2,4-dienoate

: 1379591-15-7
C₂₃H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / toluene; hexane / 3 h / -78 °C

1.2: 20 °C / pH 1 / Cooling with ice

2.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 15 h / 20 °C / Cooling with ice

3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 15 h / 0 - 20 °C

5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Inert atmosphere

5.2: 15 h / 20 °C

6.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 2 h / 20 °C

7.1: triethylamine / tetrahydrofuran / 2 h / 20 °C

7.2: 15 h / 60 °C

With hydrogenchloride; lithium aluminium tetrahydride; diphenyl phosphoryl azide; sodium hydride; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: (2E, 4E)-7-phenylhepta-2,4-dien-1-ol

: 1379591-15-7
C₂₃H₂₆N₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 15 h / 20 °C / Cooling with ice

2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 15 h / 0 - 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / Inert atmosphere

4.2: 15 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 2 h / 20 °C

6.1: triethylamine / tetrahydrofuran / 2 h / 20 °C

6.2: 15 h / 60 °C

With hydrogenchloride; lithium aluminium tetrahydride; diphenyl phosphoryl azide; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; 1,4-dioxane; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;