2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile

Base Information

Chemical Name:2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile
CAS No.:1609467-70-0
Molecular Formula:C₁₈H₁₃ClN₂O₂
Molecular Weight:324.766
Hs Code.:

Synonyms:2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile

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Chemical Property of 2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile

Chemical Property:

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Technology Process of 2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile

There total 5 articles about 2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925005-02-3
4-(4-chloro-3-methylphenoxy)benzoic acid

: 1609467-70-0
2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / tetrahydrofuran; N,N-dimethyl-formamide / 16 h / 0 - 20 °C

2.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

2.2: 3 h / Reflux

With oxalyl dichloride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 403-42-9
1-(4-fluorophenyl)ethanone

: 1609467-70-0
2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / 3 h / 100 °C

2.1: sodium hypochlorite / ethanol / 20 °C

3.1: oxalyl dichloride / tetrahydrofuran; N,N-dimethyl-formamide / 16 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

4.2: 3 h / Reflux

With sodium hypochlorite; oxalyl dichloride; sodium hydride; potassium carbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 59-50-7
4-Chloro-3-methylphenol

: 1609467-70-0
2-((4-(4-chloro-3-methylphenoxy)phenyl)(methoxy)methylene)-malononitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / 3 h / 100 °C

2.1: sodium hypochlorite / ethanol / 20 °C

3.1: oxalyl dichloride / tetrahydrofuran; N,N-dimethyl-formamide / 16 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C

4.2: 3 h / Reflux

With sodium hypochlorite; oxalyl dichloride; sodium hydride; potassium carbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;