allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

Base Information

Chemical Name:allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside
CAS No.:155711-37-8
Molecular Formula:C₃₇H₄₀Cl₆NO₁₃P
Molecular Weight:950.415
Hs Code.:

allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

Synonyms:allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

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Chemical Property of allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

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Technology Process of allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

There total 3 articles about allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 155711-36-7
allyl 6-O-benzyloxymethyl-2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 155711-37-8
allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

Guidance literature:: With pyridine; dmap; In dichloromethane; for 16h; Ambient temperature;
DOI:10.1248/cpb.41.1879

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 155711-37-8
allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 1,1,3,3-tetramethylurea / CH₂Cl₂ / 20 h / Ambient temperature

2: 89 percent / pyridine, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

With pyridine; dmap; tetramethylurea; In dichloromethane;
DOI:10.1248/cpb.44.2268

Reference yield:

: 134040-52-1
Allyl 2-deoxy-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-glucopyranoside

: 155711-37-8
allyl 6-O-benzyloxymethyl-2-deoxy-4-O-diphenylphosphono-3-O-(2,2,2-trichloro-tert-butoxycarbonyl)-2-(2,2,2-trichloroethoxycarbonylamino)-α-D-gluocopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / 1,1,3,3-tetramethylurea / CH₂Cl₂ / 20 h / Ambient temperature

2: 89 percent / pyridine, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

With pyridine; dmap; tetramethylurea; In dichloromethane;
DOI:10.1248/cpb.44.2268