di(4-methoxyphenyl) trithiocarbonate

Base Information

Chemical Name:di(4-methoxyphenyl) trithiocarbonate
CAS No.:74974-69-9
Molecular Formula:C₁₅H₁₄O₂S₃
Molecular Weight:322.473
Hs Code.:

Synonyms:di(4-methoxyphenyl) trithiocarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(4-methoxyphenyl) trithiocarbonate

Chemical Property:

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Technology Process of di(4-methoxyphenyl) trithiocarbonate

There total 2 articles about di(4-methoxyphenyl) trithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-15-0,12122-00-8
carbon disulfide

: 696-62-8
para-iodoanisole

: 74974-69-9
di(4-methoxyphenyl) trithiocarbonate

Guidance literature:: carbon disulfide; With sodium sulfide; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

para-iodoanisole; With copper(II) ferrite; In N,N-dimethyl-formamide; at 100 ℃; for 12h; Catalytic behavior;
DOI:10.1016/j.molcata.2014.02.006

Reference yield:

: 696-63-9
4-Methoxybenzenethiol

: 463-71-8
thiophosgene

: 74974-69-9
di(4-methoxyphenyl) trithiocarbonate

Guidance literature:: Multistep reaction; (i) aq. NaOH, (ii) /BRN= 1633495/;

Reference yield:

: 74974-69-9
di(4-methoxyphenyl) trithiocarbonate

: 74-88-4
methyl iodide

: 1879-16-9
1-methoxy-4-methylsulfanyl-benzene

: 77105-16-9
E-1,2-bis(methylthio)-1,2-bis(4-methoxyphenylthio)ethylene

Guidance literature:: With tetra-(n-butyl)ammonium iodide; Mechanism; Product distribution; multistep reaction: 1.) electrochemical reduction (mercury pool or platinum net; reference electrode - Ag/AgI), DMF, -10 deg C;