(R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone

Base Information

Chemical Name:(R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone
CAS No.:698353-16-1
Molecular Formula:C₁₇H₂₅NO₃
Molecular Weight:291.39
Hs Code.:

Synonyms:(R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone

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Technology Process of (R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone

There total 3 articles about (R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 698353-14-9
(2R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanol

: 698353-16-1
(R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone

Guidance literature:: With tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In dichloromethane; for 1h;
DOI:10.1139/v03-165

Reference yield:

: 100-52-7
benzaldehyde

: 698353-16-1
(R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / tetrahydrofuran; hexane / 0.25 h / -95 °C

1.2: tetrahydrofuran; hexane / 0.17 h / -95 °C

2.1: 95 percent / N-methylmorpholine-N-oxide; 4 Angstroem molecular sieves; tetrapropylammonium perruthenate / CH₂Cl₂ / 1 h

With n-butyllithium; tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1139/v03-165

Reference yield:

: 140175-19-5,140384-74-3
Methyl-((S)-2-methyl-1-tributylstannanyl-propyl)-carbamic acid tert-butyl ester

: 698353-16-1
(R)-2-(N-tert-butoxycarbonyl-N-methylamino)-3-methyl-1-phenyl-1-butanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / tetrahydrofuran; hexane / 0.25 h / -95 °C

1.2: tetrahydrofuran; hexane / 0.17 h / -95 °C

2.1: 95 percent / N-methylmorpholine-N-oxide; 4 Angstroem molecular sieves; tetrapropylammonium perruthenate / CH₂Cl₂ / 1 h

With n-butyllithium; tetrapropylammonium perruthennate; 4 A molecular sieve; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1139/v03-165