(2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate

Base Information

Chemical Name:(2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate
CAS No.:260392-69-6
Molecular Formula:C₄₄H₈₀NO₆P
Molecular Weight:750.096
Hs Code.:

Synonyms:(2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate

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Chemical Property of (2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate

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Technology Process of (2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate

There total 6 articles about (2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 60562-16-5,56270-93-0
1,2-dimyristoyl-sn-glycerol

: 108549-21-9
benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

: 260392-69-6
(2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate

Guidance literature:: With 5H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 4h; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.202114858

Reference yield:

: 73083-33-7
1-(tetradecanoyl)-3-O-benzyl-sn-glycerol

: 260392-69-6
(2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / H₂ / 10 percent Pd/C / ethyl acetate

2: 85 percent / tetrazole / 15 °C

With 1H-tetrazole; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3423::AID-ANIE3423>3.0.CO;2-I

Reference yield:

: 112-64-1
tetradecanoyl chloride

: 260392-69-6
(2R)-3-(((benzyloxy)(diisopropylamino)phosphanyl)oxy)propane-1,2-diyl ditetradecanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / pyridine

2: 80 percent / H₂ / 10 percent Pd/C / ethyl acetate

3: 85 percent / tetrazole / 15 °C

With pyridine; 1H-tetrazole; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1002/(SICI)1521-3773(19981231)37:24<3423::AID-ANIE3423>3.0.CO;2-I