2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone

Base Information

Chemical Name:2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone
CAS No.:1246814-24-3
Molecular Formula:C₄₃H₃₄O₈
Molecular Weight:678.738
Hs Code.:

Synonyms:2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone

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Chemical Property of 2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone

Chemical Property:

Purity/Quality:

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Technology Process of 2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone

There total 6 articles about 2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1246814-23-2
2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxy-2-bromoacetophenone

: 582-25-2
Potassium benzoate

: 1246814-24-3
2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone

Guidance literature:: In acetonitrile; at 82 ℃;
DOI:10.1021/acs.joc.9b03461

Reference yield:

: 18065-05-9
1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

: 1246814-24-3
2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone

Guidance literature:: Multi-step reaction with 4 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C

2: tetrahydrofuran / 4 h / 0 - 20 °C

3: phosphonic acid diethyl ester; triethylamine / tetrahydrofuran / 0 - 20 °C

4: acetonitrile / 82 °C

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; phosphonic acid diethyl ester; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/acs.joc.9b03461

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 1246814-24-3
2-benzoyloxy-2'-(4''-(benzyloxy)benzoyloxy)-4',6'-dibenzyloxyacetophenone

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 73 h

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C

3: tetrahydrofuran / 4 h / 0 - 20 °C

4: phosphonic acid diethyl ester; triethylamine / tetrahydrofuran / 0 - 20 °C

5: acetonitrile / 82 °C

With dmap; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; phosphonic acid diethyl ester; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/acs.joc.9b03461