Technology Process of 2-(3-chlorophenyl)-2-(phenylthio)acetic acid
There total 3 articles about 2-(3-chlorophenyl)-2-(phenylthio)acetic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate;
In
dimethyl sulfoxide;
at 25 ℃;
for 24h;
under 2280.15 Torr;
Irradiation;
Sealed tube;
DOI:10.1021/jacs.0c00629
- Guidance literature:
-
Multi-step reaction with 2 steps
1: methanol / 0.5 h / 60 °C
2: [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate / dimethyl sulfoxide / 24 h / 25 °C / 2280.15 Torr / Irradiation; Sealed tube
With
[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate;
In
methanol; dimethyl sulfoxide;
DOI:10.1021/jacs.0c00629
- Guidance literature:
-
Multistep reaction;
(i) SOCl2, (ii) Br2, (UV-irradiation), (iii) /BRN= 506523/, KOH;
DOI:10.1021/ja00804a027
