C₂₂H₂₃N₅O₃

Base Information

Chemical Name:C₂₂H₂₃N₅O₃
CAS No.:1346242-78-1
Molecular Formula:C₂₂H₂₃N₅O₃
Molecular Weight:405.456
Hs Code.:

C<sub>22</sub>H<sub>23</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₂H₂₃N₅O₃

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Chemical Property of C₂₂H₂₃N₅O₃

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Technology Process of C₂₂H₂₃N₅O₃

There total 11 articles about C₂₂H₂₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1346245-08-6
N-(3,5-dimethoxyphenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-3 -(1-methyl-1H-pyrazol-4-yl)-6-quinoxalinamine

: 1346242-78-1
C₂₂H₂₃N₅O₃

Guidance literature:: N-(3,5-dimethoxyphenyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-3 -(1-methyl-1H-pyrazol-4-yl)-6-quinoxalinamine; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 5h;

With water; In tetrahydrofuran; Product distribution / selectivity; Cooling with ice;

Reference yield:

: 1083325-87-4
7‐bromo‐2‐(1‐methyl‐1H‐pyrazol‐4‐yl)quinoxaline

: 1346242-78-1
C₂₂H₂₃N₅O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

2.2: 5 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C

3.2: Cooling with ice

With tetrabutyl ammonium fluoride; sodium hydride; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 89891-65-6
7-bromo-2-chloroquinoxaline

: 1346242-78-1
C₂₂H₂₃N₅O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,2-dimethoxyethane; water / 4 h / Reflux

2.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / 90 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

3.2: 5 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h / 20 °C

4.2: Cooling with ice

With tetrabutyl ammonium fluoride; sodium hydride; sodium carbonate; sodium t-butanolate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;