C₁₃H₁₇NO₂

Base Information

Chemical Name:C₁₃H₁₇NO₂
CAS No.:749189-41-1
Molecular Formula:C₁₃H₁₇NO₂
Molecular Weight:219.283
Hs Code.:

C<sub>13</sub>H<sub>17</sub>NO<sub>2</sub>

Synonyms:C₁₃H₁₇NO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₇NO₂

Chemical Property:

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Technology Process of C₁₃H₁₇NO₂

There total 1 articles about C₁₃H₁₇NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61-90-5,21675-61-6,25248-98-0,70-45-1
L-leucine

: 100-52-7
benzaldehyde

: 749189-41-1
C₁₃H₁₇NO₂

Guidance literature:: L-leucine; With lithium hydroxide monohydrate; In methanol; at 20 ℃; for 0.333333h;

benzaldehyde; In methanol; for 1h;
DOI:10.1016/j.bmcl.2011.05.123

Reference yield:

: 749189-41-1
C₁₃H₁₇NO₂

: 2743-42-2
(S)-2-(benzylamino)-4-methylpentanoic acid

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h;
DOI:10.1016/j.bmcl.2011.05.123

Reference yield:

: 749189-41-1
C₁₃H₁₇NO₂

: 1325715-68-1
1-benzyl-5-isobutyl-1H-imidazol-2-amine hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h

2.1: tetra(n-butyl)ammonium hydroxide / acetonitrile / 0.5 h / 20 °C

2.2: 18 h / 20 °C

3.1: (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

3.2: 18 h / 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / tetrahydrofuran / 1 h / -78 - 20 °C / Inert atmosphere

5.1: hydrogenchloride; water / diethyl ether / 2 h / 20 °C

6.1: CYANAMID; sodium hydroxide / ethanol; water / 3 h / 95 °C / pH 4.3

7.1: hydrogenchloride / methanol; water

With hydrogenchloride; sodium tetrahydroborate; (benzotriazol-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; CYANAMID; tetra(n-butyl)ammonium hydroxide; water; diisobutylaluminium hydride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.05.123