5,5'-Diamino-3,3'-bis-1,2,4-triazole

Base Information

• Chemical Name: 5,5'-Diamino-3,3'-bis-1,2,4-triazole
• CAS No.: 22819-10-9
• Molecular Formula: C4H6 N8
• Molecular Weight: 166.14
• Hs Code.: 2933990090
• Mol file: 22819-10-9.mol

Synonyms:3,3'-Bi-s-triazole,5,5'-diamino- (6CI,8CI); 5,5'-Diamino-3,3'-bis-1,2,4-triazole;Bis(3-amino-1,2,4-triazol-5-yl); Bis(5-amino-1,2,4-triazol-3-yl)

Chemical Property of 5,5'-Diamino-3,3'-bis-1,2,4-triazole

Chemical Property:

• Melting Point: >350 °C
• Boiling Point: 723.0±43.0 °C(Predicted)
• PKA: 8.52±0.40(Predicted)
• PSA: 136.64000
• Density: 1.870±0.06 g/cm3(Predicted)
• LogP: -1.38560

Purity/Quality:

98%min ^*data from raw suppliers

2H,2'H-3,3'-Bi-1,2,4-triazole-5,5'-diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,5'-Diamino-3,3'-bis-1,2,4-triazole

There total 6 articles about 5,5'-Diamino-3,3'-bis-1,2,4-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

aminoguanidine bicarbonate (2582-30-1) + oxalic acid (144-62-7,97993-78-7) → 1H,1′H-[3,3′-bi-1,2,4-triazole]-5,5′-diamine (22819-10-9)

Guidance literature:

aminoguanidine bicarbonate; oxalic acid; With hydrogenchloride; In water; at 70 ℃; for 1h;

With sodium hydroxide; In water; for 1h; pH=14; Reflux;

DOI:10.1002/ejic.201200221

Reference yield: 70.0%

oxalic acid (144-62-7,97993-78-7) + aminoguanidine hydrogencarbonate (2200-97-7,2582-30-1,10587-01-6,13998-67-9) → 1H,1′H-[3,3′-bi-1,2,4-triazole]-5,5′-diamine (22819-10-9)

Guidance literature:

With hydrogenchloride; In water; at 70 ℃; for 1h;

DOI:10.1002/jhet.3068

Reference yield:

5,5′-dinitro-3,3-bis-1,2,4-triazole → 1H,1′H-[3,3′-bi-1,2,4-triazole]-5,5′-diamine (22819-10-9)

Guidance literature:

With hydrogenchloride; oxalic acid; In water; for 2h; Reflux;

upstream raw materials:

oxalic acid

1-aminoguanidine hydrochloride

aminoguanidine bicarbonate

aminoguanidine hydrogencarbonate

Downstream raw materials:

3,3'-dinitro-5,5'-bis(1H-1,2,4-triazole)