p-Fluoro-(2-hydroxyhexafluoroisopropyl)benzene

Base Information

• Chemical Name: p-Fluoro-(2-hydroxyhexafluoroisopropyl)benzene
• CAS No.: 2402-74-6
• Molecular Formula: C9H5 F7 O
• Molecular Weight: 262.1242224
• Hs Code.: 2906299090
• Mol file: 2402-74-6.mol

Synonyms:Benzylalcohol, p-fluoro-a,a-bis(trifluoromethyl)- (7CI,8CI);(2-Hydroxyhexafluoro-2-propyl)-4-fluorobenzene

Chemical Property of p-Fluoro-(2-hydroxyhexafluoroisopropyl)benzene

Chemical Property:

• Boiling Point: 158℃
• PSA: 20.23000
• LogP: 3.13790

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-Fluoro-(2-hydroxyhexafluoroisopropyl)benzene

There total 2 articles about p-Fluoro-(2-hydroxyhexafluoroisopropyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

fluorobenzene (462-06-6) + Hexafluoroacetone (684-16-2) → 4-Fluor-α,α-bis-(trifluormethyl)-benzylalkohol (2402-74-6)

Guidance literature:

With aluminium trichloride;

DOI:10.1021/ja01089a020 DOI:10.1007/BF00905999

Reference yield:

Hexafluoroacetone (684-16-2) + 1-Bromo-4-fluorobenzene (460-00-4) → 4-Fluor-α,α-bis-(trifluormethyl)-benzylalkohol (2402-74-6)

Guidance literature:

With iodine; magnesium; Yield given. Multistep reaction; 1.) ether, reflux; 2.) ether, overnight;

DOI:10.1021/ja00272a050

Reference yield:

4-Fluor-α,α-bis-(trifluormethyl)-benzylalkohol (2402-74-6) → 1-fluoro-4-(perfluoropropan-2-yl)benzene (2396-25-0)

Guidance literature:

With sulfur tetrafluoride; at 150 ℃;

DOI:10.1021/ja01089a020

upstream raw materials:

Hexafluoroacetone

1-Bromo-4-fluorobenzene

fluorobenzene

Downstream raw materials:

2-bromo-2-(p-fluorophenyl)pentafluoropropane

1-(p-fluorophenyl)-1-(trifluoromethyl)-2,2,2-trifluoroethyl tosylate

1-fluoro-4-(perfluoropropan-2-yl)benzene

4-Fluor-α,α-bis-(trifluormethyl)-benzylamin

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