1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol

Base Information

Chemical Name:1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol
CAS No.:418759-61-2
Molecular Formula:C₂₂H₂₇NO₁₃
Molecular Weight:513.455
Hs Code.:

Synonyms:1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol

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Chemical Property of 1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol

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Technology Process of 1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol

There total 3 articles about 1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 418759-59-8
5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitroacetophenone

: 418759-61-2
1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 20 ℃; for 0.5h;
DOI:10.1016/S0968-0896(01)00323-6

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 418759-61-2
1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: cuprous nitrate / acetic acid; acetic anhydride

2: 92 percent / BF₃*Et₂O / CH₂Cl₂ / 13 h / 20 °C

3: 51 percent / NaBH₄ / tetrahydrofuran; ethanol / 0.5 h / 20 °C

With sodium tetrahydroborate; cuprous nitrate; boron trifluoride diethyl etherate; In tetrahydrofuran; ethanol; dichloromethane; acetic anhydride; acetic acid;
DOI:10.1016/S0968-0896(01)00323-6

Reference yield:

: 30879-49-3
1-(5-hydroxy-2-nitrophenyl)ethan-1-one

: 418759-61-2
1-[5-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-2-nitrophenyl]ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / BF₃*Et₂O / CH₂Cl₂ / 13 h / 20 °C

2: 51 percent / NaBH₄ / tetrahydrofuran; ethanol / 0.5 h / 20 °C

With sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/S0968-0896(01)00323-6