C₂₈H₂₃N

Base Information

Chemical Name:C₂₈H₂₃N
CAS No.:1426442-41-2
Molecular Formula:C₂₈H₂₃N
Molecular Weight:373.497
Hs Code.:

Synonyms:C₂₈H₂₃N

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Chemical Property of C₂₈H₂₃N

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Technology Process of C₂₈H₂₃N

There total 5 articles about C₂₈H₂₃N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 916518-57-5
5-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-1-methyl-1H-indole

: 1426442-16-1
C₂₄H₂₄O₂

: 1426442-41-2
C₂₈H₂₃N

Guidance literature:: With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; potassium tert-butylate; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; In tetrahydrofuran; toluene; butan-1-ol; at 20 ℃; for 24h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja311783k

Reference yield:

: 3218-36-8
4-Phenylbenzaldehyde

: 1426442-41-2
C₂₈H₂₃N

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylzinc / toluene / 12 h / 60 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

2.2: 23.5 h / 0 - 20 °C / Inert atmosphere

3.1: bis(1,5-cyclooctadiene)nickel⁽⁰⁾; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; potassium tert-butylate / toluene; tetrahydrofuran; butan-1-ol / 24 h / 20 °C / Inert atmosphere

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; potassium tert-butylate; diethylzinc; sodium hydride; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; butan-1-ol;
DOI:10.1021/ja311783k

Reference yield:

: [1,1′-biphenyl]-4-yl(phenyl)methanol

: 1426442-41-2
C₂₈H₂₃N

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C / Inert atmosphere

1.2: 23.5 h / 0 - 20 °C / Inert atmosphere

2.1: bis(1,5-cyclooctadiene)nickel⁽⁰⁾; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; potassium tert-butylate / toluene; tetrahydrofuran; butan-1-ol / 24 h / 20 °C / Inert atmosphere

With bis(1,5-cyclooctadiene)nickel⁽⁰⁾; potassium tert-butylate; sodium hydride; N,N'-dimesityl-4,5-dihydro-1H-imidazolium tetrafluoroborate; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; butan-1-ol;
DOI:10.1021/ja311783k