4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide

Base Information

• Chemical Name: 4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide
• CAS No.: 1470134-33-8
• Molecular Formula: C₁₉H₂₄N₈O₄S
• Molecular Weight: 460.517

Synonyms:4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide

Chemical Property of 4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide

Chemical Property:

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Technology Process of 4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide

There total 3 articles about 4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

CYANAMID (420-04-2) + 4-(6-amino-5-nitroso-4-cyclohexylmethoxypyrimidin-2-ylamino)-amino-N-methylbenzenesulfonamide (1470134-32-7) → 4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide (1470134-33-8)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In acetonitrile; at 20 ℃; for 2h;

DOI:10.1016/j.ejmech.2013.07.031

Reference yield:

2-(n-butane-1-sulfonyl)-4-cyclohexylmethoxypyrimidin-6-ylamine (651733-96-9) → 4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide (1470134-33-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 2,2,2-trifluoroethanol / 24.2 h / 20 - 80 °C

2: sodium nitrite; acetic acid / water / 1 h / 95 °C

3: [bis(acetoxy)iodo]benzene / acetonitrile / 2 h / 20 °C

With [bis(acetoxy)iodo]benzene; acetic acid; sodium nitrite; In 2,2,2-trifluoroethanol; water; acetonitrile;

DOI:10.1016/j.ejmech.2013.07.031

Reference yield:

N-methyl-4-aminobenzenesulfonamide (1709-52-0) → 4-[6-amino-5-(cyano-NNO-azoxy)-4-cyclohexylmethoxypyrimidin-2-ylamino]-amino-N-methylbenzenesulfonamide (1470134-33-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 2,2,2-trifluoroethanol / 24.2 h / 20 - 80 °C

2: sodium nitrite; acetic acid / water / 1 h / 95 °C

3: [bis(acetoxy)iodo]benzene / acetonitrile / 2 h / 20 °C

With [bis(acetoxy)iodo]benzene; acetic acid; sodium nitrite; In 2,2,2-trifluoroethanol; water; acetonitrile;

DOI:10.1016/j.ejmech.2013.07.031

upstream raw materials:

2-(n-butane-1-sulfonyl)-4-cyclohexylmethoxypyrimidin-6-ylamine

N-methyl-4-aminobenzenesulfonamide

CYANAMID

4-(6-amino-5-nitroso-4-cyclohexylmethoxypyrimidin-2-ylamino)-amino-N-methylbenzenesulfonamide

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