cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide

Base Information

Chemical Name:cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide
CAS No.:316790-80-4
Molecular Formula:C₁₄H₁₆BrNO₂
Molecular Weight:310.191
Hs Code.:

Synonyms:cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide

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Chemical Property of cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide

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Technology Process of cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide

There total 2 articles about cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 106-95-6
allyl bromide

: 316790-75-7
cyclopropanecarboxylic acid (2-bromo-4-methoxy-phenyl)-amide

: 316790-80-4
cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 8h;
DOI:10.1016/S0040-4039(00)01426-X

Reference yield:

: 32338-02-6
2-bromo-4-methoxyaniline

: 316790-80-4
cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / N,N-diisopropylethylamine / diethyl ether / 6 h / 20 °C

2: 79 percent / NaH / tetrahydrofuran / 8 h

With sodium hydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; 1: Acylation / 2: Alkylation;
DOI:10.1016/S0040-4039(00)01426-X

Reference yield: 81.0%

: 316790-80-4
cyclopropanecarboxylic acid allyl-(2-bromo-4-methoxy-phenyl)-amide

: 5-(4-methoxy-phenyl)-7-methyl-5-aza-spiro[2.4]heptan-4-one

: cyclopropyl-(5-methoxy-3-methyl-2,3-dihydro-indol-1-yl)-methanone

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 110 ℃; for 2h;
DOI:10.1016/S0040-4039(00)01426-X