Technology Process of 4'-(5,5-Dimethyl-[1,3]dioxan-2-yl)-biphenyl-4-carbaldehyde oxime
There total 3 articles about 4'-(5,5-Dimethyl-[1,3]dioxan-2-yl)-biphenyl-4-carbaldehyde oxime which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydroxylamine hydrochloride; sodium carbonate;
In
ethanol; dichloromethane; water;
Ambient temperature;
DOI:10.1246/bcsj.64.3005
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium chlorochromate, sodium acetate
2: 74 percent / hydroxylamine hydrochloride, sodium carbonate / ethanol; CH2Cl2; H2O / Ambient temperature
With
hydroxylamine hydrochloride; sodium acetate; sodium carbonate; pyridinium chlorochromate;
In
ethanol; dichloromethane; water;
DOI:10.1246/bcsj.64.3005
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) p-toluenesulfonic acid, 2.) LiAlH4 / 1.) benzene, reflux, 2 h, 2.) THF
2: pyridinium chlorochromate, sodium acetate
3: 74 percent / hydroxylamine hydrochloride, sodium carbonate / ethanol; CH2Cl2; H2O / Ambient temperature
With
lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; sodium carbonate; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
ethanol; dichloromethane; water;
DOI:10.1246/bcsj.64.3005
