(S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate
CAS No.:120369-51-9
Molecular Formula:C₁₇H₂₆N₂O₃S
Molecular Weight:338.471
Hs Code.:

Synonyms:(S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate

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Chemical Property of (S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate

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Technology Process of (S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate

There total 3 articles about (S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 2488-15-5
N-tert-butoxycarbonyl-L-methionine

: 100-46-9
benzylamine

: 120369-51-9
(S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate

Guidance literature:: With bis(cyclopentadienyl)hafnium dichloride; In diethyl ether; at 26 ℃; for 48h; Molecular sieve;
DOI:10.1021/acscatal.5b00385

Reference yield: 80.0%

: 33900-24-2
N-(tert-butoxycarbonyl)-L-methionine methyl ester

: 100-46-9
benzylamine

: 120369-51-9
(S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate

Guidance literature:: With 4-hydroxybenzotrifluoride; sodium methylate; In toluene; at 50 ℃; for 99h; optical yield given as %ee; Inert atmosphere; Molecular sieve;
DOI:10.1039/c2cc32153j

Reference yield: 50.0%

: 120369-51-9
(S)-tert-butyl 1-(benzylamino)-4-(methylthio)-1-oxobutan-2-ylcarbamate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; for 0.5h; Cooling with ice;

With 4-methyl-morpholine; In tetrahydrofuran; at 20 ℃; for 12h; pH=8;