BENZOHYDROXAMIC ACID SODIUM SALT

Base Information

• Chemical Name: BENZOHYDROXAMIC ACID SODIUM SALT
• CAS No.: 22513-32-2
• Molecular Formula: C7H7 N O2 . Na
• Molecular Weight: 159.12
• Mol file: 22513-32-2.mol

Synonyms:Benzamide,N-hydroxy-, monosodium salt (9CI); Benzohydroxamic acid sodium salt (6CI);Benzohydroxamic acid, monosodium salt (8CI); Sodium benzohydroxamate

Chemical Property of BENZOHYDROXAMIC ACID SODIUM SALT

Chemical Property:

• PSA: 52.16000
• LogP: 1.30510
• Water Solubility.: almost transparency

Purity/Quality:

98%,99%, ^*data from raw suppliers

SodiumBenzohydroxamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZOHYDROXAMIC ACID SODIUM SALT

There total 4 articles about BENZOHYDROXAMIC ACID SODIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.6%

benzoic acid methyl ester (93-58-3,5705-52-2,80226-58-0) → acid sodium salt of benzohydroxamic acid (22513-32-2)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; at 40 - 50 ℃; for 4h; Reagent/catalyst; Temperature;

Reference yield: 88.91%

diethyleneglycol dibenzoate (120-55-8,9004-86-8) → acid sodium salt of benzohydroxamic acid (22513-32-2)

Guidance literature:

With hydroxylamine hydrochloride; sodium hydroxide; at 33 ℃; for 0.25h; Temperature;

Reference yield: 87.0%

dibenzoyl peroxide (94-36-0) → acid sodium salt of benzohydroxamic acid (22513-32-2)

Guidance literature:

dibenzoyl peroxide; With sodium hydrogensulfite; In tetrahydrofuran; for 0.333333h;

With hydroxylamine hydrochloride; sodium hydroxide; In tetrahydrofuran; for 3h; Solvent;

upstream raw materials:

diethyleneglycol dibenzoate

1,2-ethanediol, dibenzoate

benzoic acid methyl ester

dibenzoyl peroxide

Downstream raw materials:

N-(prop-2-yn-1-yloxy)benzamide

oxo bis-benzhydroxamato vanadium (IV)

trisodium tris(benzohydroximato)cobaltate(III)*5H₂O

tris(benzohydroxamato)cobalt(III)*1.5H₂O

Refernces

• 1、 -. "Carboxylic ester oximationmethod". Paragraph 0055-0057; 0060-0062; 0084-0086. . Retrieved 2019/11/04.