oxo bis-benzhydroxamato vanadium (IV)

Base Information

• Chemical Name: oxo bis-benzhydroxamato vanadium (IV)
• CAS No.: 14708-33-9
• Molecular Formula: C₁₄H₁₂N₂O₅V
• Molecular Weight: 339.201
• Mol file: 14708-33-9.mol

Synonyms:

Chemical Property of oxo bis-benzhydroxamato vanadium (IV)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of oxo bis-benzhydroxamato vanadium (IV)

There total 2 articles about oxo bis-benzhydroxamato vanadium (IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

oxovanadium(IV) sulfate + acid sodium salt of benzohydroxamic acid (22513-32-2) → oxo bis-benzhydroxamato vanadium (IV) (14708-33-9)

Guidance literature:

In water; room temp.;; digested on a water-bath for 0.5 h; filtered; washed with hot water and ether; dried in vacuo; elem. anal.;;

Reference yield:

oxovanadium(IV) sulfate + potassium benzohydroxamate (32685-16-8) → oxo bis-benzhydroxamato vanadium (IV) (14708-33-9)

Guidance literature:

In water; reaction at pH 3 - 4 on heating;; crystallization; washing with H2O and drying in vacuum over CaCl2;;

Reference yield: 60.0%

oxo bis-benzhydroxamato vanadium (IV) (14708-33-9) → (oxo)bis(benzhydroxamato)(2,2'-bipyridine)vanadium(IV)

Guidance literature:

With 2,2'-bipyridyl; In methanol; benzene; ligand in benzene added to complex in dry MeOH; refluxed for 0.5 h;; concd.; crystals dried in vacuo at room temp.; elem. anal.;;

upstream raw materials:

acid sodium salt of benzohydroxamic acid

potassium benzohydroxamate

Downstream raw materials:

oxo methoxo bis-benzhydroxamato vanadium (V)

Refernces