Dispiro[5.1.5.1]tetradecane-7,14-dithione

Base Information

Chemical Name:Dispiro[5.1.5.1]tetradecane-7,14-dithione
CAS No.:22502-49-4
Molecular Formula:C14H20 S2
Molecular Weight:0
Hs Code.:
DSSTox Substance ID:DTXSID60499097
Wikidata:Q82349593
Mol file:22502-49-4.mol

Synonyms:Dispiro[5.1.5.1]tetradecane-7,14-dithione;22502-49-4;DTXSID60499097;FT-0625344;Dispiro[5.1.5~8~.1~6~]tetradecane-7,14-dithione

Suppliers and Price of Dispiro[5.1.5.1]tetradecane-7,14-dithione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DISPIRO[5.1.5.1]TETRADECANE-7,14-DITHIONE 95.00%
5MG
$ 495.14

Total 3 raw suppliers

Chemical Property of Dispiro[5.1.5.1]tetradecane-7,14-dithione

Chemical Property:

Refractive Index:1.616
PSA：64.18000
LogP:4.64080
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:252.10064299
Heavy Atom Count:16
Complexity:277

Purity/Quality:

99% ^*data from raw suppliers

DISPIRO[5.1.5.1]TETRADECANE-7,14-DITHIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC2(CC1)C(=S)C3(C2=S)CCCCC3

Technology Process of Dispiro[5.1.5.1]tetradecane-7,14-dithione

There total 6 articles about Dispiro[5.1.5.1]tetradecane-7,14-dithione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 950-21-0
dispiro[5.1.5.1]tetradecane-7,14-dione

: 22502-48-3
1,4-thioxodispiro[5.1.5⁸.1⁶]tetradecan-7-one

: 22502-49-4
Dispiro<5.1.5.1>tetradecane-7,14-dithione

Guidance literature:: With hydrogenchloride; hydrogen sulfide; zinc(II) chloride; In methanol; ethanol;
DOI:10.1021/jo00387a007

Reference yield: 45.0%

: 22502-48-3
1,4-thioxodispiro[5.1.5⁸.1⁶]tetradecan-7-one

: 22502-49-4
Dispiro<5.1.5.1>tetradecane-7,14-dithione

Guidance literature:: With tetraphosphorus decasulfide; In pyridine; for 2h; Heating;
DOI:10.1021/jo00172a008

Reference yield:

: 950-21-0
dispiro[5.1.5.1]tetradecane-7,14-dione

: 22502-49-4
Dispiro<5.1.5.1>tetradecane-7,14-dithione

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / P₂S₅ / pyridine / 2 h / Heating

2: 45 percent / P₂S₅ / pyridine / 2 h / Heating

With tetraphosphorus decasulfide; In pyridine;
DOI:10.1021/jo00172a008