[1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

Base Information

Chemical Name:[1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane
CAS No.:1030891-88-3
Molecular Formula:C₁₆H₁₅Br₂F₅Si
Molecular Weight:490.181
Hs Code.:

Synonyms:[1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

Suppliers and Price of [1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

Chemical Property:

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Technology Process of [1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

There total 3 articles about [1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 558-13-4
carbon tetrabromide

: 1030892-23-9
1-pentafluorophenyl-3-tert-butyldimethylsilylpropynone

: 1030891-88-3
[1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

Guidance literature:: With triphenylphosphine; In dichloromethane; for 3h; Inert atmosphere;
DOI:10.1021/ol800583r

Reference yield:

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: 1030891-88-3
[1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 0 °C

2: triphenylphosphine / dichloromethane / 0 °C

With aluminum (III) chloride; triphenylphosphine; In dichloromethane; 1: Friedel Crafts acylation;
DOI:10.1055/s-0029-1217706

Reference yield:

: 107474-01-1
(tert-butyldimethylsilyl)(trimethylsilyl)acetylene

: 1030891-88-3
[1,1-dibromo-3-(pentafluorophenyl)but-1-en-3-ynyl]-tert-butyldimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 0 °C

2: triphenylphosphine / dichloromethane / 0 °C

With aluminum (III) chloride; triphenylphosphine; In dichloromethane; 1: Friedel Crafts acylation;
DOI:10.1055/s-0029-1217706