2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide

Base Information

Chemical Name:2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide
CAS No.:1416235-79-4
Molecular Formula:C₄₃H₄₇N₃O₁₅S
Molecular Weight:877.923
Hs Code.:

Synonyms:2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide

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Chemical Property of 2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide

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Technology Process of 2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide

There total 7 articles about 2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 98-59-9
p-toluenesulfonyl chloride

: 620127-95-9
2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylate-ethoxy]ethoxy}ethoxy)ethyl]benzo[lmn]-[3,8]phenanthroline,1,3,6,8-tetraone

: 1416235-79-4
2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide

Guidance literature:: 2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylate-ethoxy]ethoxy}ethoxy)ethyl]benzo[lmn]-[3,8]phenanthroline,1,3,6,8-tetraone; With silver(l) oxide; In dichloromethane; at 0 ℃; for 1h;

p-toluenesulfonyl chloride; With potassium iodide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1039/c2ob26587g

Reference yield:

: 112-60-7
Tetraethylene glycol

: 1416235-79-4
2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide

Guidance literature:: Multi-step reaction with 6 steps

1.1: silver(l) oxide / dichloromethane

1.2: 12 h / 0 - 20 °C

2.1: sodium azide / N,N-dimethyl-formamide / 4 h / 110 °C

3.1: triphenylphosphine / tetrahydrofuran / 12 h / 0 - 20 °C

3.2: 12 h

4.1: N,N-dimethyl-formamide / 0.08 h / Microwave irradiation

5.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane; tetrahydrofuran / 12 h

6.1: silver(l) oxide / dichloromethane / 1 h / 0 °C

6.2: 0 - 20 °C

With sodium azide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; triphenylphosphine; silver(l) oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26587g

Reference yield:

: 65883-12-7
2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethyl methanesulfonate

: 1416235-79-4
2-[2-(2-{2-[2-nicotinoyloxyethoxy]ethoxy}ethoxy)ethyl]-7-[2-(2-{2-[2-tosylethoxy]ethoxy}ethoxy)ethyl]-1,4,5,8-naphthalenedicarboxiimide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide / N,N-dimethyl-formamide / 4 h / 110 °C

2.1: triphenylphosphine / tetrahydrofuran / 12 h / 0 - 20 °C

2.2: 12 h

3.1: N,N-dimethyl-formamide / 0.08 h / Microwave irradiation

4.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane; tetrahydrofuran / 12 h

5.1: silver(l) oxide / dichloromethane / 1 h / 0 °C

5.2: 0 - 20 °C

With sodium azide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; triphenylphosphine; silver(l) oxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob26587g