methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

Base Information

Chemical Name:methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside
CAS No.:109200-42-2
Molecular Formula:C₁₈H₂₄N₆O₇
Molecular Weight:436.425
Hs Code.:

Synonyms:methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

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Chemical Property of methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

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Technology Process of methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

There total 10 articles about methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83030-01-7
methyl 2-azido-3-O-benzyl-2-deoxy-α-D-xylopyranoside

: 109200-42-2
methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) silver perchlorate, 2,4,6-trimethylpyridine, Drierite / 1.) nitromethane, -10 degC, 1 h; 2.) nitromethane, -10 degC, 60 h

2: sodium methoxide / methanol

With 2,4,6-trimethyl-pyridine; calcium sulfate; sodium methylate; silver perchlorate; In methanol;
DOI:10.1246/bcsj.59.3137

Reference yield:

: 83022-17-7
methyl 4-O-(3,4-di-O-acetyl-2-azido-2-deoxy-β-D-xylopyranosyl)-2-azido-3-O-benzyl-2-deoxy-α-D-xylopyranoside

: 109200-42-2
methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

Guidance literature:: DOI:10.1016/S0040-4039(00)87195-6

Reference yield:

: 83022-09-7
3,4-di-O-acetyl-2-azido-2-deoxy-α-D-xylopyranosyl chloride

: 109200-42-2
methyl 2-azido-4-O-(2-azido-2-deoxy-β-D-xylopyranosyl)-3-O-benzyl-2-deoxy-α-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) silver perchlorate, 2,4,6-trimethylpyridine, Drierite / 1.) nitromethane, -10 degC, 1 h; 2.) nitromethane, -10 degC, 60 h

2: sodium methoxide / methanol

With 2,4,6-trimethyl-pyridine; calcium sulfate; sodium methylate; silver perchlorate; In methanol;
DOI:10.1246/bcsj.59.3137